HuagongsheHuagongshe Chemistry Print Report · For research reference only
4'-Methoxy-3-nitro-biphenyl-4-malonate → 4'-Methoxy-3-nitrobiphenyl-4-acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4'-Methoxy-3-nitro-biphenyl-4-malonate | HCID 21925763 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 4'-Methoxy-3-nitrobiphenyl-4-acetic acid | HCID 10493503 | — |
Reaction Steps
Crude 4′-methoxy-3-nitro-biphenyl-4-malonate was heated at 100° C. in 60 mL of 6N hydrochloric acid for 15 hours and cooled. The precipitate was collected by filtration, washed with water and hexane, and dried to give 7.2 g of crude 4′-methoxy-3-nitrobiphenyl-4-acetic acid as a light tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06706709B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-f88c80a779da411fabf953662200c5dd |
| Source note | uspto-grants-2004_03 |