HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butylbenzoyl chloride → 4-tert-butyl-N-(2,3-dibromophenyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butylbenzoyl chloride | HCID 74372 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 2,3-Dibromobenzenamine | HCID 15579998 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 4-tert-butyl-N-(2,3-dibromophenyl)benzamide | HCID 57678294 | — |
Reaction Steps
The amide was prepared according to Example 18 from 2,3-dibromoaniline, 4-tert-butylbenzoyl chloride and diisopropylethylamine in dioxane. MS (ESI) m/z 408; HPLC Method B, purity 80.6% at 210-370 nm, 11.4 min.; 74.9% at 240 nm, 11.4 min.; HRMS: calcd for C17H17Br2NO+H+, 409.97496; found (ESI, [M+H]+), 409.9775.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07531542B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-abd9a5dbcd4f462f933b1e234c1bc8b2 |
| Source note | uspto-grants-2009_05 |