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HRID491427

反应详情

EQUATION

反应方程式

HRID 491427 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C)c1ccc(C(=O)Cl)cc1
HCID74372

Benzoyl chloride, 4-(1,1-dimethylethyl)-

C11H13ClO

结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：Nc1cccc(Br)c1Br
HCID15579998

2,3-Dibromobenzenamine

C6H5Br2N

PRODUCTS

生成物

1
结构：CC(C)(C)c1ccc(C(=O)Nc2cccc(Br)c2Br)cc1
HCID57678294

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

The amide was prepared according to Example 18 from 2,3-dibromoaniline, 4-tert-butylbenzoyl chloride and diisopropylethylamine in dioxane. MS (ESI) m/z 408; HPLC Method B, purity 80.6% at 210-370 nm, 11.4 min.; 74.9% at 240 nm, 11.4 min.; HRMS: calcd for C17H17Br2NO+H+, 409.97496; found (ESI, [M+H]+), 409.9775.

WORKUP

后处理

  1. customat 210-370 nm, 11.4 min.
  2. customat 240 nm, 11.4 min.