Dansyl chloride → (4aS,8aR)-4-(3,4-Dimethoxyphenyl)-2-[1-(5-dimethylamino-naphthalene-1-sulfonyl)-piperidin-4-yl]-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one

関与物質

役割	名称	HCID	仕込み量
反応物	Dansyl chloride	HCID 11801	—
反応物	(4aS,8aR)-4-(3,4-Diethoxyphenyl)-2-[1-(toluene-4-sulfonyl)-piperidin-4-yl]-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one	HCID 10175016	—
生成物	(4aS,8aR)-4-(3,4-Dimethoxyphenyl)-2-[1-(5-dimethylamino-naphthalene-1-sulfonyl)-piperidin-4-yl]-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one	HCID 10153262	—

Prepared from dansylchloride and starting compound A1 as described for compound 1. Crystallisation from methanol. M.p. 198-200° C.