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HRID491444

反应详情

EQUATION

反应方程式

HRID 491444 的结构方程式

REACTANTS

反应物

3
结构：O
HCID962

Water

H2O

结构：Cl.ClCc1ccncc1
HCID74570

4-(Chloromethyl)pyridinium chloride

C6H7Cl2N

结构：COc1ccc(C2=NN(C3CCN(c4ccc([N+](=O)[O-])cc4)CC3)C(=O)[C@@H]3CC=CC[C@H]23)cc1OC
HCID10128150

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C2=NN(C3CCN(Cc4ccncc4)CC3)C(=O)[C@@H]3CC=CC[C@H]23)cc1OC
HCID10310661

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

Prepared from starting compound A1 and 4-picolylchloride hydrochloride as described for compound 11. After the addition of 100 ml of water, 20 ml of diethyl ether is added and the resulting mixture stirred for 30 min. The precipitate is filtered off and dried. M.p. 196-197° C.

WORKUP

后处理

  1. customPrepared
  2. additionis added
  3. filtrationThe precipitate is filtered off
  4. customdried