HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 10310661, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4-(Chloromethyl)pyridinium chloride | HCID 74570 | — |
| Reactant | HCID 10128150 | HCID 10128150 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 10310661 | HCID 10310661 | — |
Reaction Steps
Prepared from starting compound A1 and 4-picolylchloride hydrochloride as described for compound 11. After the addition of 100 ml of water, 20 ml of diethyl ether is added and the resulting mixture stirred for 30 min. The precipitate is filtered off and dried. M.p. 196-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07531540B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-b2a75a745b7040b18cd50e808abc4437 |
| Source note | uspto-grants-2009_05 |