Benzyl Isothiocyanate → HCID 11602594, compound

HRID 491693Notes

Reaction equation

[CH2:1]([N:8]=[C:9]=[S:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:11]12([N:21]=[C:22]=[O:23])[CH2:20][CH:15]3[CH2:16][CH:17]([CH2:19][CH:13]([CH2:14]3)[CH2:12]1)[CH2:18]2.C([O:26]CC)C>>[C:11]12([N:21]3[C:22](=[O:23])[N:8]([CH2:1][C:2]4[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=4)[C:9](=[O:26])[S:10]3)[CH2:20][CH:15]3[CH2:16][CH:17]([CH2:19][CH:13]([CH2:14]3)[CH2:12]1)[CH2:18]2

Participants

Reactant 3

HCID 2346Benzyl Isothiocyanate

HCID 3283Diethyl Ether

HCID 20599951-Isocyanatoadamantane

Product 1

HCID 11602594HCID 11602594, compound

Procedure

Reagents: Benzylisothiocyanate (6.5 mmol, 0.85 mL), 1-Adamantyl-isocyanate (6.5 mmol, 1.15 g) and SO2Cl2 (6.5 mmol, 0.52 mL) in diethyl ether (25 mL). Isolation: solvent evaporation.

Workup

customIsolation: solvent evaporation

Sources & evidence

ORD record: ord-f79ca526d4d64b65bad90f5703d2ea56
Source dataset: uspto-grants-2009_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07531561B2

Reaction notes

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