2,5-Dimethoxyaniline → HCID 135528624, compound

HRID 491708Notes

Reaction equation

HRID 491708 reaction equation
[CH3:1][O:2][C:3]1[CH:9]=[CH:8][C:7]([O:10]C)=[CH:6][C:4]=1[NH2:5].[Cl:12][C:13]1[CH:21]=[C:20]([O:22]C)[CH:19]=[CH:18][C:14]=1C(O)=O>>[Cl:12][C:13]1[CH:21]=[C:20]([OH:22])[CH:19]=[CH:18][C:14]=1[C:1]1[O:2][C:3]2[CH:9]=[CH:8][C:7]([OH:10])=[CH:6][C:4]=2[N:5]=1

Participants

3

Reactant 2

HCID 76132,5-DimethoxyanilineHCID 126480262-Chloro-4-methoxybenzoic acid

Product 1

HCID 135528624HCID 135528624, compound

Procedure

The title compound was prepared in substantially the same manner as described in Example 1, from 2,5-dimethoxyaniline, and 2-chloro-4-methoxybenzoic acid and was obtained as a white solid, m.p. 253-255° C.; MS m/e 262 (M+H)+.

Workup

  1. customwas obtained as a white solid, m.p. 253-255° C.

Sources & evidence

ORD record
ord-7800bb73532147a2bc06800785e39294
Source dataset
uspto-grants-2009_05
Patent number
US07531564B2

Reaction notes

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