2,4-Dimethoxyaniline → HCID 135493215, compound

HRID 491711Notes

Reaction equation

HRID 491711 reaction equation
[CH3:1][O:2][C:3]1[CH:9]=[C:8]([O:10]C)[CH:7]=[CH:6][C:4]=1[NH2:5].C[O:13][C:14]1[CH:22]=[CH:21][C:20]([O:23]C)=[CH:19][C:15]=1C(O)=O>>[OH:10][C:8]1[CH:7]=[CH:6][C:4]2[N:5]=[C:1]([C:21]3[CH:22]=[C:14]([OH:13])[CH:15]=[CH:19][C:20]=3[OH:23])[O:2][C:3]=2[CH:9]=1

Participants

3

Reactant 2

HCID 176522,4-DimethoxyanilineHCID 760272,5-Dimethoxybenzoic acid

Product 1

HCID 135493215HCID 135493215, compound

Procedure

The title compound was prepared in substantially the same manner as described in Example 1, from 2,4-dimethoxyaniline, and 2,5-dimethoxybenzoic acid and was obtained as a tan solid, m.p. 278-280° C.; MS m/e 244 (M+H)+.

Workup

  1. customwas obtained as a tan solid, m.p. 278-280° C.

Sources & evidence

ORD record
ord-6b9f7acdb9b6452ebea10a59c7b792b5
Source dataset
uspto-grants-2009_05
Patent number
US07531564B2

Reaction notes

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