HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53904438, compound → Tropenol 2-fluoro-2,2-diphenylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53904438 | HCID 53904438 | — |
| Reactant | Tropenol benzilate | HCID 86585680 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | Tropenol 2-fluoro-2,2-diphenylacetate | HCID 86585679 | — |
Reaction Steps
15.86 ml (0.086 mol) of bis-(2-methoxyethyl)-aminosulphur trifluoride are reacted with 25 g (0.072 mol) of 5f analogously to Example 4, step 4.3 in 480 ml of chloroform. The product is recrystallised from acetone in the form of its hydrochloride. Yield: 18.6 g of white crystals (=67% of theory);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06706726B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-ab215f0c7cc14b3b9dc804990fbbf00b |
| Source note | uspto-grants-2004_03 |