反应详情

温度

80 °C

1.58 g (10.0 mmol) of phenylphosphonic acid (manufactured by Nissan Chemical industries, Ltd.), 0.583 g (10.0 mmol) of magnesium hydroxide and 41 g of water were mixed, stirred at 80° C. for 3 hours, then water was distilled off under reduced pressure and dried at 200° C. to obtain 1.78 g (yield 99%) of the aimed product as white crystal. Decomposition temperature: 524° C.

1. distillationwater was distilled off under reduced pressure
2. customdried at 200° C.