HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 57678987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 57679000 | HCID 57679000 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57678987 | HCID 57678987 | — |
Reaction Steps
[(6-Benzenesulfonylamino-naphthalen-1-ylmethyl)-amino]-acetic acid ethyl ester is added to methylamine in methanol, and the solution is stirred at room temperature, then concentrated under reduced pressure. The oil is dissolved in ethanol and 1N HCl in diethyl ether is added to precipitate 2-[(6-benzenesulfonyl-naphthalen-1-ylmethyl)-amino]-N-methyl-acetamide as a hydrochloride salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07531577B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-a9348aec42f1420894b75dfc24901c10 |
| Source note | uspto-grants-2009_05 |