Triethylamine → HCID 66593908, compound

HRID 492101Notes

Reaction equation

HRID 492101 reaction equation
[CH3:1][C:2]1[CH:6]([CH3:7])[CH:5]=[C:4]([CH3:8])[C:3]=1[C:9]1[CH:14]=[C:13]([CH3:15])[CH:12]=[C:11]([CH3:16])[C:10]=1[NH2:17].C(N(CC)CC)C.[C:25](Cl)(=[O:30])[C:26]([CH3:29])([CH3:28])[CH3:27]>>[CH3:1][C:2]1[CH:6]([CH3:7])[CH:5]=[C:4]([CH3:8])[C:3]=1[C:9]1[CH:14]=[C:13]([CH3:15])[CH:12]=[C:11]([CH3:16])[C:10]=1[NH:17][C:25](=[O:30])[C:26]([CH3:29])([CH3:28])[CH3:27]

Participants

4

Reactant 3

HCID 8471TriethylamineHCID 62493Pivaloyl chlorideHCID 66593770HCID 66593770, compound

Product 1

HCID 66593908HCID 66593908, compound

Procedure

2-(2,3,5-trimethylcyclopenta-1,4-dienyl)-4,6-dimethylphenyl(trimethylacetyl)a mine was prepared in the same manner as Example 11, except that 0.600 g (2.64 mmol) of 2-(2,3,5-trimethylcyclopenta-1,4-dienyl)-4,6-dimethylphenylamine, 0.321 g (3.17 mmol) of triethylamine, and 0.382 g (3.17 mmol) of pivaloyl chloride were used (0.727 g, 89%).

Sources & evidence

ORD record
ord-620294625a1346f8b60b70306a4ec1c1
Source dataset
uspto-grants-2009_05
Patent number
US07531608B2

Reaction notes

Loading…