HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentylamine → HCID 12071574, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentylamine | HCID 8060 | — |
| Reactant | phenyl 2,4,6-trimethylphenylcarbamate | HCID 691608 | — |
| Reactant | 5-(4'-(Bromomethyl)(1,1'-biphenyl)-2-yl)-1-trityl-1H-tetraazole | HCID 10053461 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 12071574 | HCID 12071574 | 22% |
Reaction Steps
Using n-pentylamine (304.2 mg), triethylamine (442.2 mg), [[2′-(N-(triphenylmethyl)tetrazol-5-yl]-1,1′-biphenyl-4-yl]methyl] bromide (400 mg) and phenyl 2,4,6-trimethylphenylcarbamate (233.8 mg), N′-pentyl-N-(2,4,6-trimethylphenyl)-N′-[[2′-[N-(triphenylmethyl)tetrazol-5-yl]-1,1′-biphenyl-4-yl]methyl]urea (113 mg) was obtained by a similar procedure as in Example 1. Yield: 22%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07531576B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-d6a134d493ce4578ab94455a2350b8a8 |
| Source note | uspto-grants-2009_05 |