HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178418675, compound → 3-Oxabicyclo[3.2.2]nonane-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178418675 | HCID 178418675 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | 3-Oxabicyclo[3.2.2]nonane-2,4-dione | HCID 14097169 | 97% |
Reaction Steps
A solution of 2.9 g of cis-cyclohexane-1,4-dicarboxylic acid in 25 ml of acetic anhydride was heated under reflux for 2.5 hours. The solvent was removed by evaporation in vacuo, and the residue was triturated under diethyl ether several times. The residue was dried under high vacuum to give 2.5 g (97% yield) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05242911 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-9551d7b99ad4419ca95993482a6ed9e7 |
| Source note | uspto-grants-1993_09 |