HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 4'-hydroxy-4-biphenylcarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Propylbenzoic acid | HCID 137601 | — |
| Reactant | 4'-Hydroxy-4-biphenylcarboxylic acid | HCID 301556 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ethyl 4'-hydroxy-4-biphenylcarboxylate | HCID 4049156 | — |
Reaction Steps
The reaction was conducted in the same manner as in the step (i) of the Example 33, except for using 4-(4-hydroxyphenyl)benzoic acid and ethanol in lieu of 4-n-propylbenzoic acid and methanol, respectively, and the resultant was recrystallized from toluene to give ethyl 4-(4-hydroxyphenyl)benzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07534547B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-9202b041f1b14830b03a07aa49b22dea |
| Source note | uspto-grants-2009_05 |