HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 57681491, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 67074012 | HCID 67074012 | — |
| Catalyst | Benzyl triethylammonium chloride | HCID 66133 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57681491 | HCID 57681491 | — |
Reaction Steps
To a solution of 29.15 g (0.0587 mol) of 2-bromo-1-{4-[4-(2-bromo-2-methyl-propionyl)-phenoxy]-phenyl}-2-ethyl-butane-1-one dissolved in 60 ml of dichloromethane, 16.88 g (0.211 mol) of 50% NaOH and 291.5 mg of 50% BTEAC were added. The reaction was refluxed for 3 h, adding every 30′, 291.5 mg of BTEAC, then diluted with water and dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07534880B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-297892acd2e148c2836bf05eeb225c8e |
| Source note | uspto-grants-2009_05 |