HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphenyl Ether → HCID 67073672, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphenyl Ether | HCID 7583 | — |
| Reactant | 2-Bromo-2-methylpropionyl bromide | HCID 88685 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67073672 | HCID 67073672 | — |
Reaction Steps
7.82 g of AlCl3 were added in about 30′ to a solution of 10 g (0.0587 mol) of diphenylether and 7.44 ml (0.0587 mol) of α-bromoisobutyrylbromide (97.5% w/w) in 100 ml of dichloromethane, maintaining the temperature between 0 e 5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07534880B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-48dc9b1a463144da8421c084cb8929a9 |
| Source note | uspto-grants-2009_05 |