Hydrogen Bromide → HCID 67073671, compound

Participants

Reaction Steps

A drop of 48% HBr was added to a solution of 11.95 g (26.83 mmol) of 2-bromo-1-[4-(4-cyclohexancarbonyl-phenylsulphanyl)-phenyl]-2-methyl-propan-1-one dissolved in 120 ml of dichloromethane; in 15′ 1.37 ml (26.83 mmol) of bromine dissolved in 10 ml of dichloromethane were added drop wise. After 1 h the organic phase was washed with water and with a sodium metabisulphite solution. The organic phase was separated, washed with brine, dried with sodium sulphate, filtered and evaporated under vacuum obtaining 14.07 g of a yellowish oil.

Provenance & Evidence