HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphenyl Ether → HCID 67073672, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphenyl Ether | HCID 7583 | — |
| Reactant | 2-Bromo-2-methylpropionyl bromide | HCID 88685 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67073672 | HCID 67073672 | — |
Reaction Steps
39.19 g of aluminium trichloride (0.294 mol) were added, between 0° C. and 5° C. In 45′ to a solution of 50 g of diphenylether (0.294 mol) and 37.27 ml of α-bromoisobutyrylbromide in 250 ml of dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07534880B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-ec9576515fee497381c55ae395c46ade |
| Source note | uspto-grants-2009_05 |