HRID493447

反应详情

EQUATION

反应方程式

HRID 493447 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

One equivalent of 40% by weight of sodium hydroxide in water was mixed with one equivalent of benzyl mercaptan with R-22 (1.1 molar equivalents) at 60° C. for 1 h. The tests are carried out in a 500 ml Hastelloy reactor at an autogenous pressure at 60° C. The pressure is 3.5 bar. A chemical yield of 75%, by quantitative determination by 19F NMR, is obtained over two tests carried out under the same conditions.

WORKUP

后处理

  1. customThe tests are carried out in a 500 ml Hastelloy reactor at an autogenous pressure at 60° C
  2. customA chemical yield of 75%, by quantitative determination by 19F NMR, is obtained over two tests