HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 2(1H)-Quinoxalinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Product | 2(1H)-Quinoxalinone | HCID 14526 | — |
Reaction Steps
A mixture of the 1,2-phenylene-diamine derivative (1 g) and the 2-oxo-carboxylic acid derivative (1 eq) in dry EtOH (35 mL) was stirred at reflux for 2 h under nitrogen. After cooling, the EtOH was evaporated to give a crude brown solid. Recrystallisation from EtOH gave the desired quinoxalin-2-one derivative.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538109B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-e11bf6e15ac14fa9a03e91a18f60a7dd |
| Source note | uspto-grants-2009_05 |