HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 6428849, compound → 1,5-Dimethylpiperazin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 6428849 | HCID 6428849 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 1,5-Dimethylpiperazin-2-one | HCID 20806335 | — |
Reaction Steps
A mixture of 1,5-dimethylpyrazin-2(1H)-one (5.7 g, 45.9 mmol) and platinum oxide (0.57 g) in ethyl acetate (100 mL) was stirred under an atmosphere of hydrogen (1 atm) at room temperature overnight. The product mixture was filtered through a pad of Celite, and concentrated under vacuum to provide 1,5-dimethyl-piperazin-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538112B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-3fc24955cc784791a1dd1fc5b9340386 |
| Source note | uspto-grants-2009_05 |