HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → 2-Methoxy-N-quinolin-7-yl-1,1'-biphenyl-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 4-bromo-3-methoxy-N-quinolin-7-ylbenzamide | HCID 69042670 | — |
| Product | 2-Methoxy-N-quinolin-7-yl-1,1'-biphenyl-4-carboxamide | HCID 57682698 | — |
Reaction Steps
Using the procedure outlined in Example 58, the title compound was prepared from 4-bromo-3-methoxy-N-quinolin-7-ylbenzamide (D69) (76 mg, 0.21 mmol) and phenylboronic acid (28 mg, 0.23 mmol) as a white solid. MS(ES): MH+ 355, M-H+ 353.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538121B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-045557b01b2a467f93ec528345cefeca |
| Source note | uspto-grants-2009_05 |