Hydrochloric Acid → HCID 68829620, compound

Participants

Reaction Steps

To a stirred solution of Example 37 (100 mg, 0.30 mmol) in EtOAc (3 ml) was added a saturated solution of dry HCl in EtOAc (2 ml). This solution was stirred at RT for 30 min to result a white precipitate. The product was collected by filtration and dried under vacuum to give 112 mg of the product as a white solid; 1H NMR (D2O, 300 MHz) δ 1.44-1.64 (m, 2H), 1.81-2.06 (m, 2H), 2.11-2.37 (m, 7H), 2.60-2.62 (m, 1H), 3.45-3.77 (m, 4H), 4.18-4.38 (m, 2H), 4.40-4.44 (m, 2H), 8.52 (s, 1H), 9.23 (s, 1H).

Provenance & Evidence