HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(2-Methyl-3-nitrophenyl)acetic acid → HCID 57683265, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(2-Methyl-3-nitrophenyl)acetic acid | HCID 13530897 | — |
| Edukt | HCID 57683249 | HCID 57683249 | — |
| Katalysator | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Produkt | HCID 57683265 | HCID 57683265 | 89,7% |
Reaktionsschritte
The 2-methyl-3-nitrophenylacetic acid (307 mg) obtained in Example 5c), 4-dimethylaminopyridine (217 mg) and the 2-(2-hydroxyethyl)-2-phenylmalonic acid diethyl ester (250 mg) obtained in Example 5e) were subjected to reactions similar to those in Example 1-3c) to give the title compound (366 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07538140B2 |
| Quelldatensatz | uspto-grants-2009_05 |
| ORD ID | ord-d026ed1a4cdc49de8455c6bcd22cab1c |
| Quellennotiz | uspto-grants-2009_05 |