HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58907415, compound → HCID 23032549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58907415 | HCID 58907415 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23032549 | HCID 23032549 | — |
Reaction Steps
A suspension of methyl (2E)-3-[3-(2-oxopropyl)phenyl]acrylate (5.00 g, Preparation 138) and 10% palladium on carbon (500 mg) in ethanol (50 ml) was stirred under an atmosphere of hydrogen (60 psi) at room temperature for 16 hours. The catalyst was filtered off through arbocel and the filtrate concentrated in vacuo to give the title compound as a pale yellow oil which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538141B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-99e7778a94b74c049042f6311b63187b |
| Source note | uspto-grants-2009_05 |