HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Malonate → Dimethyl 2-(2-isopentyl-5-methyl-2-phenylhexanoyl)malonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Malonate | HCID 7761 | — |
| Reactant | 2-Phenyl-2-propylpentanoyl chloride | HCID 11687335 | — |
| Reactant | 2-isopentyl-5-methyl-2-phenylhexanoyl Chloride | HCID 86598020 | — |
| Product | Dimethyl 2-(2-isopentyl-5-methyl-2-phenylhexanoyl)malonate | HCID 69270654 | — |
Reaction Steps
The title compound was prepared following the procedure of Example 1E, substituting dimethyl malonate for diethyl malonate, and substituting the product of Example 6D for the product of Example 1D. 1H NMR (300 MHz, CDCl3): δ 7.32 (m, 5 H), 4.54 (s, 1 H), 3.56 (s, 6 H), 2.00 (m, 4 H), 1.49 (m, 2 H), 0.87 (m, 16 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538105B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-899e710a521e460ca2b43c92637f89f4 |
| Source note | uspto-grants-2009_05 |