Sodium Hydroxide → HCID 25260422, compound

Participants

Reaction Conditions

Reaction Steps

A suspension of the product of Example 40I (2.12 g) in water (10 mL) and treated with 0.997N sodium hydroxide solution (0.969 mL, 0.966 mmol) and stirred at 25° C. for 1 hour. The solution was lyophilized to give the title compound (0.412 g, 79%). 1H NMR (300 MHz, DMSO-d6): δ ppm 0.46 (m, 1H) 0.69 (m, 6H) 0.80 (m, 1H) 1.29 (m, 1H) 1.38 (m, 3H) 1.72 (m, 1H) 2.14 (m, 1H) 2.90 (m, 3H) 7.34 (m, 6H) 8.05 (m, 1H) 15.42 (m, 1H). MS (ESI−) m/z 516 (M−H)−.

Provenance & Evidence