Hydrochloric Acid → HCID 136384866, compound

Participants

Reaction Steps

A solution of Example 41G (1.44, 2.56 mmol) in 4M hydrochloric acid in 1,4-dioxane (10 mL) was stirred at 25° C. for 1 hour. The solution was concentrated in vacuo and the residue was triturated in diethyl ether to give the title compound (1.17 g, 91%). 1H NMR (300 MHz, DMSO-d6): δ ppm 0.78 (m, 7H) 1.35 (m, 7H) 2.20 (m, 2H) 7.02 (m, 2H) 7.50 (m, 2H) 7.76 (m, 2H) 8.16 (m, 1H) 13.61 (m, 1H).

Provenance & Evidence