HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 66593465, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-Mesitylenesulfonyl chloride | HCID 13046 | — |
| Reactant | HCID 66593777 | HCID 66593777 | — |
| Product | HCID 66593465 | HCID 66593465 | — |
Reaction Steps
0.700 g (3.25 mmol) of 2-(2-amino-5-methylphenyl)-3-methyl-2-cyclopenten-1-one, 0.283 g (3.58 mmol) of pyridine, 0.782 g (3.58 mmol) of 2-mesitylenesulfonyl chloride, and 3 mL of M.C were loaded to a 20 mL vial, and then reacted for 12 hours. The work-up was the same as in Example 7 (1.29 g, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538239B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-804a24e08e7340dc91e86e6c6c13d8a1 |
| Source note | uspto-grants-2009_05 |