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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 495158Generated: October 29, 2026

Pyridine → HCID 66593465, compound

https://huagongshe.com/reaction/495158

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
Reactant2-Mesitylenesulfonyl chlorideHCID 13046—
ReactantHCID 66593777HCID 66593777—
ProductHCID 66593465HCID 66593465—

Reaction Steps

0.700 g (3.25 mmol) of 2-(2-amino-5-methylphenyl)-3-methyl-2-cyclopenten-1-one, 0.283 g (3.58 mmol) of pyridine, 0.782 g (3.58 mmol) of 2-mesitylenesulfonyl chloride, and 3 mL of M.C were loaded to a 20 mL vial, and then reacted for 12 hours. The work-up was the same as in Example 7 (1.29 g, 85%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07538239B2
Source datasetuspto-grants-2009_05
ORD IDord-804a24e08e7340dc91e86e6c6c13d8a1
Source noteuspto-grants-2009_05