HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 66593512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | HCID 66593931 | HCID 66593931 | — |
| Product | HCID 66593512 | HCID 66593512 | 89% |
Reaction Steps
An experiment was performed in the same manner as in Example 49 using 0.534 g (2.68 mmol) of 2-(2,3,5-trimethylcyclopenta-1,4-dienyl)phenylamine, 0.325 g (3.22 mmol) of triethylamine, and 0.388 g (3.22 mmol) of pivaloyl chloride. The reaction product was purified using a column chromatography with a hexane/ethylacetate (v/v, 5:1) solvent. The purified product was dried in vacuum to remove the solvent therein, thereby obtaining while solid (0.674 g, 89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538239B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-fede89a18d7c4f2d932342bed22e679a |
| Source note | uspto-grants-2009_05 |