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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 495168Generated: October 30, 2026

Triethylamine → HCID 66593512, compound

https://huagongshe.com/reaction/495168

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantPivaloyl chlorideHCID 62493—
ReactantHCID 66593931HCID 66593931—
ProductHCID 66593512HCID 6659351289%

Reaction Steps

An experiment was performed in the same manner as in Example 49 using 0.534 g (2.68 mmol) of 2-(2,3,5-trimethylcyclopenta-1,4-dienyl)phenylamine, 0.325 g (3.22 mmol) of triethylamine, and 0.388 g (3.22 mmol) of pivaloyl chloride. The reaction product was purified using a column chromatography with a hexane/ethylacetate (v/v, 5:1) solvent. The purified product was dried in vacuum to remove the solvent therein, thereby obtaining while solid (0.674 g, 89%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07538239B2
Source datasetuspto-grants-2009_05
ORD IDord-fede89a18d7c4f2d932342bed22e679a
Source noteuspto-grants-2009_05