HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 86619915, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Bis(4-methoxyphenyl)phosphinic acid | HCID 624223 | — |
| Reactant | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86619915 | HCID 86619915 | — |
Reaction Steps
To a flask were added 2.0 g bis(4-methoxyphenyl)phosphinic acid, 3.0 g of a 55-60% solution of tetrabutylammonium hydroxide in water, 2.0 g of water and 18 ml 2-propanol. After heating to 50 C under nitrogen for 1 hour, the solvent was removed and another 20 ml of 2-propanol were added and removed by distillation under reduced pressure. A waxy solid was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538931B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-5cd1fe7a1e804b33aa0912df3eab481a |
| Source note | uspto-grants-2009_05 |