Formaldehyde → HCID 11314307, compound

Participants

Reaction Steps

Compound 1 (0.19 g, 0.74 mmol) obtained in Example 1 was dissolved in 2-propanol (3.0 mL), and morpholine (0.065 mL, 0.75 mmol) and aqueous 37% formalin solution (0.063 mL, 0.78 mmol) were added thereto and stirred at room temperature for 4 hours. The reaction solution was concentrated under reduced pressure, and then purified through preparative thin-layer chromatography (methanol/chloroform=1/9) to obtain Compound 14 (0.091 g, 35%) as a colorless oily substance.

Provenance & Evidence