HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-(1-methylpiperidin-4-ylidene)acetate → Methyl 2-(1-methylpiperidin-4-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-(1-methylpiperidin-4-ylidene)acetate | HCID 20672702 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Methyl 2-(1-methylpiperidin-4-yl)acetate | HCID 19425952 | — |
Reaction Steps
(1-Methyl-piperidin-4-ylidene)-acetic acid methyl ester (Step A) was stirred under H2 overnight (1.1 g of 10% Pd/C and 200 mL EtOH), filtered and evaporated to give (1-methyl-piperidin-4-yl)-acetic acid methyl ester as a yellow oil/white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06939874B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-dacca3ed436b4d0f94be5b29df70d83f |
| Source note | uspto-grants-2005_09 |