HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → HCID 69796510, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | HCID 14629888 | HCID 14629888 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69796510 | HCID 69796510 | 86.3% |
Reaction Steps
To a solution of D2 (12.7 g, 0.036 mol) and cyclohexene (excess, 20 ml) in ethanol (100 ml) was added 10% palladium on charcoal catalyst. Reaction was heated at reflux overnight and cooled. Catalyst was filtered and the filtrate concentrated to leave an oil (6.69 g) which was used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06939891B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-aa3eccba618748809eeaaf288611ce69 |
| Source note | uspto-grants-2005_09 |