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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 495962Generated: October 31, 2026

HCID 22461733, compound → HCID 21339496, compound

https://huagongshe.com/reaction/495962

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22461733HCID 22461733—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
SolventMethanolHCID 887—
ProductHCID 21339496HCID 21339496—

Reaction Steps

A solution of 1-1 (7.360 g, 21.87 mmol) in methanol (200 mL) was added to a suspension of 10% palladium on carbon in ethanol (100 mL). The mixture was stirred under hydrogen gas pressure at room temperature for 3 hours. The reaction mixture was filtered through celite and the filtrate evaporated in vacuo to afford the title compound 1-2 as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06943156B2
Source datasetuspto-grants-2005_09
ORD IDord-e3e816261f3b459bbe1edda35f7319ac
Source noteuspto-grants-2005_09