HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22461733, compound → HCID 21339496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22461733 | HCID 22461733 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21339496 | HCID 21339496 | — |
Reaction Steps
A solution of 1-1 (7.360 g, 21.87 mmol) in methanol (200 mL) was added to a suspension of 10% palladium on carbon in ethanol (100 mL). The mixture was stirred under hydrogen gas pressure at room temperature for 3 hours. The reaction mixture was filtered through celite and the filtrate evaporated in vacuo to afford the title compound 1-2 as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06943156B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-e3e816261f3b459bbe1edda35f7319ac |
| Source note | uspto-grants-2005_09 |