HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 495964Generated: October 30, 2026
HCID 13000267, compound → HCID 20689155, compound
https://huagongshe.com/reaction/495964
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 13000267 | HCID 13000267 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20689155 | HCID 20689155 | — |
Reaction Steps
A solution of 1-3 (1.16 g, 4.80 mmol) in THF (50 mL) was treated with a solution of 1M LiAlH4 in THF (10.0 mL, 10.0 mmol) and heated to 55° C. for 2 hours. The reaction was quenched with aqueous ammonium chloride and extracted with diethyl ether. The solvents were removed in vacuo to afford 1-4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06943156B2 |
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| Source dataset | uspto-grants-2005_09 |
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| ORD ID | ord-a658356483df482a9139e60fbb2e4979 |
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| Source note | uspto-grants-2005_09 |
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