HRID496054

反应详情

EQUATION

反应方程式

HRID 496054 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1.45 liters of 1N sodium hydroxide solution are added to a solution, cooled to 5° C., of 1.45 ml of methyl 1,1-cyclopropanedicarboxylate in 2.5 liters of methanol. After stirring for 4 days at ambient temperature, the mixture is three-quarters concentrated, extracted with ether and then treated in customary manner, allowing the expected product to be isolated.

WORKUP

后处理

  1. concentrationconcentrated
  2. extractionextracted with ether
  3. additiontreated in customary manner
  4. customto be isolated