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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 496070Generated: October 30, 2026

Potassium Iodide → HCID 70142752, compound

https://huagongshe.com/reaction/496070

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium IodideHCID 4875—
ReactantPotassium CyanideHCID 9032—
ReactantSodium CarbonateHCID 10340—
ReactantHCID 70144582HCID 70144582—
SolventDimethyl SulfoxideHCID 679—
SolventWaterHCID 962—
ProductHCID 70142752HCID 70142752—

Reaction Conditions

Temperature70 °C

Reaction Steps

A mixture containing 26.4 g of the product of Step 1, 26 g of potassium cyanide and 2.6 g of potassium iodide in 264 ml of dimethyl sulphoxide is stirred at 70° C. for 20 hours. The mixture is cooled and 400 ml of 10% sodium carbonate in water are added. After extraction with ether and customary treatment, evaporation of the residue under reduced pressure allows the expected product to be isolated.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06943184B2
Source datasetuspto-grants-2005_09
ORD IDord-bce5ee0717b84928912e06d7d6e8fba0
Source noteuspto-grants-2005_09