HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 9942941, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 17840539 | HCID 17840539 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 9942941 | HCID 9942941 | — |
Reaction Steps
20 ml of 4N hydrochloric acid in dioxane are added to a mixture containing 4.4 g of the product obtained in Step 2 in 20 ml of dioxane. Stirring is carried out for 4 hours at 20° C. and then 20 ml of ether are added. Crystallisation is observed. The crystals are filtered off, washed with ether and dried at 50° C. and 0.5 torr, allowing the expected product to be obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06943184B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-bd17b48e48e74149bd8023b94bce11f4 |
| Source note | uspto-grants-2005_09 |