HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11278269, compound → HCID 69742386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11278269 | HCID 11278269 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69742386 | HCID 69742386 | — |
Reaction Steps
16 g (0.0518 mol) of the preceding derivative (4) dissolved in 600 ml of ethanol was hydrogenated in the presence of palladium-on-charcoal under a hydrogen pressure of 8 bar. After filtering off the catalyst, the expected derivative (5) was isolated in the form of the hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06946005B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-fe33e128ca304317b042b5e670a9cbdf |
| Source note | uspto-grants-2005_09 |