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HRID496539

反应详情

EQUATION

反应方程式

HRID 496539 的结构方程式

REACTANTS

反应物

2
结构：CC(C)CCC(=O)Cl
HCID170008

Pentanoyl chloride, 4-methyl-

C6H11ClO

结构：CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1ccco1
HCID4393688

2-(Tributylstannyl)furan

C16H30OSn

PRODUCTS

生成物

1
结构：CC(C)CCC(=O)c1ccco1
HCID95287

1-Pentanone, 1-(2-furanyl)-4-methyl-

C10H14O2

AUXILIARIES

试剂、催化剂与溶剂

2
结构：Cl[Pd](Cl)([P](c1ccccc1)(c1ccccc1)c1ccccc1)[P](c1ccccc1)(c1ccccc1)c1ccccc1
催化剂HCID178418476

未命名化合物

结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

A solution of 2-tributylstannylfuran (1 mmol), 4-methylvaleroyl chloride (1.1 mmol), and PdCl2(PPh3)2 (0.05 mmol) in THF was stirred at 25° C. for 24 h. Extraction and chromatography gave 2-(4-methylvaleryl)furan.

WORKUP

后处理

  1. extractionExtraction and chromatography