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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 496745Generated: October 26, 2026

N,N'-bis-(2-amino-ethyl)-N,N'-dimethyl-propane-1,3-diamine → 3-chloro-6-{2-[(3-{[2-(3-chloro-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-ylamino)-ethyl]-methyl-amino}-propyl)-methyl-amino]-ethylamino}-5,10-diaza-benzo[c]fluoren-7-one

https://huagongshe.com/reaction/496745

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN,N'-bis-(2-amino-ethyl)-N,N'-dimethyl-propane-1,3-diamineHCID 10607670—
Reactanttoluene-4-sulfonic acid 3-chloro-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-yl esterHCID 20829787—
Product3-chloro-6-{2-[(3-{[2-(3-chloro-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-ylamino)-ethyl]-methyl-amino}-propyl)-methyl-amino]-ethylamino}-5,10-diaza-benzo[c]fluoren-7-oneHCID 10417414—

Reaction Steps

In a similar manner to Example 4, this compound was obtained starting from toluene-4-sulfonic acid 3-chloro-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-yl ester (the compound of Reference Example 7c-1) and N,N′-bis-(2-amino-ethyl)-N,N′-dimethyl-propane-1,3-diamine. The desired product was obtained as a reddish powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06946472B2
Source datasetuspto-grants-2005_09
ORD IDord-0f0fe11fc3ca4bef8447589fff63755d
Source noteuspto-grants-2005_09