HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-bis-(2-amino-ethyl)-N,N'-dimethyl-propane-1,3-diamine → 3-chloro-6-{2-[(3-{[2-(3-chloro-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-ylamino)-ethyl]-methyl-amino}-propyl)-methyl-amino]-ethylamino}-5,10-diaza-benzo[c]fluoren-7-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-bis-(2-amino-ethyl)-N,N'-dimethyl-propane-1,3-diamine | HCID 10607670 | — |
| Reactant | toluene-4-sulfonic acid 3-chloro-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-yl ester | HCID 20829787 | — |
| Product | 3-chloro-6-{2-[(3-{[2-(3-chloro-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-ylamino)-ethyl]-methyl-amino}-propyl)-methyl-amino]-ethylamino}-5,10-diaza-benzo[c]fluoren-7-one | HCID 10417414 | — |
Reaction Steps
In a similar manner to Example 4, this compound was obtained starting from toluene-4-sulfonic acid 3-chloro-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-yl ester (the compound of Reference Example 7c-1) and N,N′-bis-(2-amino-ethyl)-N,N′-dimethyl-propane-1,3-diamine. The desired product was obtained as a reddish powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06946472B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-0f0fe11fc3ca4bef8447589fff63755d |
| Source note | uspto-grants-2005_09 |