HRID496746

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10607670

未命名化合物

结构：COc1ccc2c3c(c(OS(=O)(=O)c4ccc(C)cc4)nc2c1C)C(=O)c1ccnc(Cl)c1-3

HCID20829788

未命名化合物

PRODUCTS

生成物

结构：COc1ccc2c3c(c(NCCN(C)CCCN(C)CCNc4nc5c(C)c(OC)ccc5c5c4C(=O)c4ccnc(Cl)c4-5)nc2c1C)C(=O)c1ccnc(Cl)c1-3

HCID10440385

未命名化合物

PROCEDURE

实验过程

In a similar manner to Example 4, this compound was obtained starting from toluene-4-sulfonic acid 11-chloro-3-methoxy-4-methyl-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-yl ester (the compound of Reference Example 5) and N,N′-bis-(2-amino-ethyl)-N,N′-dimethyl-propane-1,3-diamine. The desired product was obtained as a reddish powder.

WORKUP

后处理

customIn a similar manner to Example 4, this compound was obtained

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-beb4baff74c5490692df59351259275c
来源数据集: uspto-grants-2005_09
DOI: 10.6084/m9.figshare.5104873.v1
专利: US06946472B2
来源说明: uspto-grants-2005_09

反应 SMILES

[Cl:1][C:2]1[C:3]2[C:4]3[C:5]4[CH:30]=[CH:29][C:28]([O:31][CH3:32])=[C:27]([CH3:33])[C:6]=4[N:7]=[C:8](OS(C4C=CC(C)=CC=4)(=O)=O)[C:9]=3[C:10](=[O:15])[C:11]=2[CH:12]=[CH:13][N:14]=1.[NH2:34][CH2:35][CH2:36][N:37]([CH3:46])[CH2:38][CH2:39][CH2:40][N:41]([CH2:43][CH2:44][NH2:45])[CH3:42]>>[Cl:1][C:2]1[C:3]2[C:4]3[C:5]4[CH:30]=[CH:29][C:28]([O:31][CH3:32])=[C:27]([CH3:33])[C:6]=4[N:7]=[C:8]([NH:45][CH2:44][CH2:43][N:41]([CH2:40][CH2:39][CH2:38][N:37]([CH2:36][CH2:35][NH:34][C:8]4[C:9]5[C:10](=[O:15])[C:11]6[CH:12]=[CH:13][N:14]=[C:2]([Cl:1])[C:3]=6[C:4]=5[C:5]5[CH:30]=[CH:29][C:28]([O:31][CH3:32])=[C:27]([CH3:33])[C:6]=5[N:7]=4)[CH3:46])[CH3:42])[C:9]=3[C:10](=[O:15])[C:11]=2[CH:12]=[CH:13][N:14]=1