HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-bis-(2-amino-ethyl)-N,N'-dimethyl-propane-1,3-diamine → 11-chloro-6-{2-[(3-{[2-(11-chloro-3-methoxy-4-methyl-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-ylamino)-ethyl]-methyl-amino}-propyl)-methylamino]-ethylamino}-3-methoxy-4-methyl-5,10-diaza-benzo[c]fluoren-7-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-bis-(2-amino-ethyl)-N,N'-dimethyl-propane-1,3-diamine | HCID 10607670 | — |
| Reactant | toluene-4-sulfonic acid 11-chloro-3-methoxy-4-methyl-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-yl ester | HCID 20829788 | — |
| Product | 11-chloro-6-{2-[(3-{[2-(11-chloro-3-methoxy-4-methyl-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-ylamino)-ethyl]-methyl-amino}-propyl)-methylamino]-ethylamino}-3-methoxy-4-methyl-5,10-diaza-benzo[c]fluoren-7-one | HCID 10440385 | — |
Reaction Steps
In a similar manner to Example 4, this compound was obtained starting from toluene-4-sulfonic acid 11-chloro-3-methoxy-4-methyl-7-oxo-7H-5,10-diaza-benzo[c]fluoren-6-yl ester (the compound of Reference Example 5) and N,N′-bis-(2-amino-ethyl)-N,N′-dimethyl-propane-1,3-diamine. The desired product was obtained as a reddish powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06946472B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-beb4baff74c5490692df59351259275c |
| Source note | uspto-grants-2005_09 |