反应详情

温度

60 °C

A solution of 20.0 g (81.5 mmol) of 2-methylsulfanyl-4′-nitrobiphenyl in 150 ml of glacial acetic acid is treated with 66 g of sodium perborate trihydrate and heated at 60° C. with stirring for 3 days. The reaction mixture is added to water, and the precipitate is filtered off and recrystallized from petroleum ether/ethyl acetate. A yellowish solid is obtained; FAB 278

1. filtrationthe precipitate is filtered off
2. customrecrystallized from petroleum ether/ethyl acetate
3. customA yellowish solid is obtained