HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15551922, compound → 4-(2-Methylsulfonylphenyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15551922 | HCID 15551922 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 4-(2-Methylsulfonylphenyl)aniline | HCID 10800516 | — |
Reaction Steps
A solution of 17.0 g (61.3 mmol) of 2-methanesulfonyl-4′-nitrobiphenyl in 170 ml of THF is treated with 3.5 g of THF-moist Raney nickel and hydrogenated at room temperature and normal pressure until the completion of hydrogen absorption (18 hours). The catalyst is filtered off and the filtrate is evaporated. A colourless solid is obtained; FAB 248
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06946489B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-b1fca8ac2d2347f9932cded2963bac23 |
| Source note | uspto-grants-2005_09 |