反应详情

A solution of 17.0 g (61.3 mmol) of 2-methanesulfonyl-4′-nitrobiphenyl in 170 ml of THF is treated with 3.5 g of THF-moist Raney nickel and hydrogenated at room temperature and normal pressure until the completion of hydrogen absorption (18 hours). The catalyst is filtered off and the filtrate is evaporated. A colourless solid is obtained; FAB 248

1. customnormal pressure until the completion of hydrogen absorption (18 hours)
2. filtrationThe catalyst is filtered off
3. customthe filtrate is evaporated
4. customA colourless solid is obtained