HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → HCID 22323115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 3-Cyanophenol | HCID 13394 | — |
| Reactant | Ethyl 2-bromovalerate | HCID 79071 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 22323115 | HCID 22323115 | — |
Reaction Steps
A solution of 5.0 g (42 mmol) of 3-hydroxybenzonitrile and 8.78 g (42.0 mmol) of ethyl 2-bromovalerate in 80 ml of acetonitrile is treated with 13.7 g (42.0 mmol) of caesium carbonate and stirred at room temperature for 18 hours. The reaction mixture is filtered off and the filtrate evaporated. A colourless oil is obtained; FAB 248
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06946489B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-f11b29b50631449ba176e1175d25ae60 |
| Source note | uspto-grants-2005_09 |